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This document specifies methods for the chemical analysis of fine high purity barium titanate powders used as the raw material for fine ceramics.
This document stipulates the determination methods of the barium, titanium, aluminium, cadmium, calcium, cobalt, dysprosium, iron, lead, magnesium, manganese, nickel, niobium, potassium, silicon, sodium, strontium, vanadium, zirconium, carbon and oxygen contents in high purity barium titanate powders. The barium and titanium contents, the major elements, are determined by using an acid decomposition-gravimetric method or an acid decomposition-inductively coupled plasma-optical emission spectrometry (ICP-OES) method. The aluminium, cadmium, calcium, chromium, cobalt, dysprosium, iron, lead, magnesium, manganese, nickel, potassium, silicon, strontium, vanadium and zinc contents are simultaneously determined via an acid digestion-ICP-OES method. The oxygen content is determined via an inert gas fusion-IR absorption spectrometry method. Finally, the carbon content is determined using a combustion-IR absorption spectrometry method or a combustion-thermal conductometry method.
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